Geometric phase analysis is a method of digital signal processing used to determine crystallographic quantities such as d-spacing or strain from high-resolution transmission electron microscope images.[1][2] The analysis needs to be performed using specialized computer program.
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Transcription
Principle
In geometric phase analysis, crystallographic quantities are not determined at one particular point of the input image. Instead, they are quantified across the whole image resulting in a two-dimensional map of given quantity. Quantities which can be mapped with geometric phase analysis include interplanar distances (d-spacing), strain tensor and displacement vector.
Since the calculations are performed in frequential domain, the input image of crystal lattice must be transformed into frequential representation using Fourier transform. From mathematical point of view, the frequential image is a complex matrix with the size equal to the original image. From crystallographic point of view, it can be seen as an artificial diffraction pattern or reciprocal image as it depicts reciprocal lattice. In this representation, the intensity peaks (or power peaks) correspond to the crystallographic planes depicted in the original image.
Due to the complex nature of the frequential image, it can be used to calculate amplitude and phase. Together with a vector of one crystallographic plane depicted in the image, the amplitude and phase can be used to generate a 2D map of d-spacing.[1] If two vectors of non-parallel planes are known, the method can be used to generate maps of strain and displacement.[2]
Software
In order to perform geometric phase analysis, a computer tool is needed. Firstly, because manual evaluation of transforms between spatial and frequential domain would be highly impractical. Secondly, a vector of crystallographic plane is an important input parameter and the analysis is sensitive to the accuracy of its localization. Therefore, the accuracy and repeatability of the analysis can be increased by an automated localization of diffraction spots.
The required functionalities are available in crystallographic suite CrysTBox. It offers an interactive implementation geometric phase analysis called gpaGUI. Within gpaGUI, it is possible to index the diffraction spots and localize them with sub-pixel precision using an automated tool diffractGUI.[3]
- High-resolution image of magnesium processed with geometric phase analysis.
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Input image (magnesium) -
Filtered image of plane (0 1 0) -
Map of (0 1 0) d-spacing -
Map of XX component of strain tensor -
Map of X component of displacement vector
See also
- High-resolution transmission electron microscopy
- Fourier transform
- Transmission electron microscope
- CrysTBox
References
- ^ a b Hÿtch, M.J. (1997). "Geometric phase analysis of high resolution electron microscope images". Scanning Microscopy. 11: 53–66.
- ^ a b Hÿtch, M.J.; Snoeck, E.; Kilaas, R. (1998). "Quantitative measurement of displacement and strain fields from HREM micrographs". Ultramicroscopy. Elsevier BV. 74 (3): 131–146. doi:10.1016/s0304-3991(98)00035-7. ISSN 0304-3991.
- ^ Klinger, Miloslav (2017-07-07). "More features, more tools, more CrysTBox". Journal of Applied Crystallography. International Union of Crystallography (IUCr). 50 (4): 1226–1234. doi:10.1107/s1600576717006793. ISSN 1600-5767.
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This page was last edited on 27 November 2023, at 04:59